Head of the Laboratory
Kodess Michael Isaakovich
Phone: +7 (343) 341-57-55; 362-34-02; внутр. 46-71; 44-02

Staff

Dr. Olga V. Koryakova, Researcher, Ph.D.

Marina A. Yozhikova, Junior Researcher

Evgeniya G. Matochkina, Leading Engineer

Valery Z. Shaburov, Leading Service Engineer

Investigation lines

Structural studies on the wide range of organic compounds including element-containing, heterocyclic and bioorganic ones using NMR and IR techniques.

Investigations of the reaction mechanisms based on the study of kinetics and transition state structures.

Identification and certification of organic compounds.

Equipment:

NMR spectroscopy:

Bruker DRX-400 spectrometer (Bruker AG, Germany), operating frequency 400 MHz. The instrument is supplied with broad band (BBO) and inverse (BBI) NMR probes.

BS-587A spectrometer (Tesla, Czech Republic), operating frequency 80 MHz.
The available instrumentation makes it possible to perform all kinds of the advanced experiments in the field of high resolution NMR including:
- Registration of 1D spectra of almost all magnetic active isotopes including various double resonance techniques;
- 2D homo- and hetero-nuclear correlation spectroscopy;
- 1D NOE difference spectroscopy;
- Measurements of relaxation times T1 and T2.

IR spectroscopy:

Spectrum One (Perkin Elmer, USA). Spectral range 7800 - 370 cm^-1

Specord 75 IR (Carl-Zeiss Jena, Germany). Spectral range 4000-400 cm^-1

Specord M80 (Carl-Zeiss Jena, Germany). Spectral range 4000-400 cm^-1
All spectrophotometers are equipped with cells to perform the measurements at elevated temperatures (up to 250 °C) in an inert atmosphere.

UV spectroscopy:

UV-2600 (Shimadzu, Japan) Spectral range 190-1400 nm.

NMR Group is incorporated into Ural Regional NMR Spectroscopy Center ("Ural-NMR") which is financially supported by RFBR.